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2
.gitignore
vendored
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2
.gitignore
vendored
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dist
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node_modules
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.refsrc.json
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23
.refsrc.json
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{
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"title": "flt QRH",
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"description": "{{description}} 网站说明",
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"keywords": "关键字,refs-cli,refs,cli",
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"data-info": "👆 需要你的参与",
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"search": {
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"label": "搜索",
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"placeholder": "搜索备忘清单",
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"cancel": "取消"
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},
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"editor": {
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"disabled": true
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},
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"github": {
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"url": "https://github.com/flt6"
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},
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"home": {
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"label": "首页",
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"url": "https://www.flt6.com"
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},
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// "footer": "<br />备案号:支持HTML字符串",
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"license": "All rights reserved. Copyright © 2026 flt6"
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}
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BIN
docs/assets/26041901.png
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docs/assets/26041901.png
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docs/assets/26041902.jpg
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docs/assets/26041902.jpg
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docs/实验.md
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docs/实验.md
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实验备忘
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===
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## 冷冻干燥
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<!--rehype:body-class=cols-2-->
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### 开机
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- 在群里预约
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- 将样品送227冷冻过夜
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- 于249插电启动设备
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- 按下【冷冻】按钮,预冷30min或温度下到-50℃
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- 在接近完成时取出样品
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- 打开盖子放入样品后盖好压紧
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- 取下管子,放入左侧凹槽
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- 点击【真空计】后点击【真空泵】
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- 真空计下到25后即可。
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<!--rehype:className=style-timeline-->
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**如果冷冻意外中断,需等待30min后重新进行。**<!--rehype:style=color: red;-->
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### 关机
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- 插管并点击【真空泵】关闭
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- 压力下降后,点击【冷冻】关闭
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- 关机拔电
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- 打开盖子取出样品
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<!--rehype:className=style-timeline-->
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## 吸附测试
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<!--rehype:body-class=cols-2-->
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### 吸附
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- 取微球10mg,误差允许0.2mg
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- 取Re 20ppm溶液10mL
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- 加入后摇床24h准时取出(35.1℃ 180rpm)
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- 过滤,保留微球和滤液
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<!--rehype:className=style-timeline-->
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### 浓度测试-显色反应
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- 去离子水洗,润洗后,移取1mL待测样品
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- 移取5mL 6M盐酸
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- 移液枪移取0.5mL SnCl2和0.5mL 20% NH4SCH
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- 静置20min
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- 移取5mL乙酸乙酯
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- 静置10min
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<!--rehype:className=style-timeline-->
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### 分光光度准备
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- 前往310,带乙酸乙酯,比色皿,样品,手纸,吸管
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- 电脑开机设备开机
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- 电脑启动UV Probe
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- 基线800-200,自动调零
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- 放入乙酸乙酯样品于前后端
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<img
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src="assets/26041901.png"
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alt="alt text"
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width="200"
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/>
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- 基线800-200,自动调零
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- Ctrl-M 附件 6连池
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- 进入【光度测量】
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- 进入【自动调零】
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<!--rehype:className=style-timeline-->
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### 分光光度测量
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- 打开`E:/lele/铼标准曲线`
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- 样品表写id写1,2,3...
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<img
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src="assets/26041902.jpg"
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alt="alt text"
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width="200"
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/>
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- 【读取Unk】
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<!--rehype:className=style-timeline-->
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