diff --git a/.gitignore b/.gitignore
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+++ b/.gitignore
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+dist
+node_modules
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diff --git a/.refsrc.json b/.refsrc.json
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+++ b/.refsrc.json
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+{
+  "title": "flt QRH",
+  "description": "{{description}} 网站说明",
+  "keywords": "关键字,refs-cli,refs,cli",
+  "data-info": "👆 需要你的参与",
+  "search": {
+    "label": "搜索",
+    "placeholder": "搜索备忘清单",
+    "cancel": "取消"
+  },
+  "editor": {
+    "disabled": true
+  },
+  "github": {
+    "url": "https://github.com/flt6"
+  },
+  "home": {
+    "label": "首页",
+    "url": "https://www.flt6.com"
+  },
+  // "footer": "<br />备案号：支持HTML字符串",
+  "license": "All rights reserved. Copyright © 2026 flt6"
+}
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diff --git a/docs/实验.md b/docs/实验.md
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+++ b/docs/实验.md
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+实验备忘
+===
+
+## 冷冻干燥
+<!--rehype:body-class=cols-2-->
+
+
+### 开机 
+
+- 在群里预约
+- 将样品送227冷冻过夜
+- 于249插电启动设备
+- 按下【冷冻】按钮，预冷30min或温度下到-50℃
+- 在接近完成时取出样品
+- 打开盖子放入样品后盖好压紧
+- 取下管子，放入左侧凹槽
+- 点击【真空计】后点击【真空泵】
+- 真空计下到25后即可。
+<!--rehype:className=style-timeline-->
+
+**如果冷冻意外中断，需等待30min后重新进行。**<!--rehype:style=color: red;-->
+
+### 关机
+
+- 插管并点击【真空泵】关闭
+- 压力下降后，点击【冷冻】关闭
+- 关机拔电
+- 打开盖子取出样品
+<!--rehype:className=style-timeline-->
+
+## 吸附测试
+<!--rehype:body-class=cols-2-->
+
+
+### 吸附
+
+- 取微球10mg，误差允许0.2mg
+- 取Re 20ppm溶液10mL
+- 加入后摇床24h准时取出（35.1℃ 180rpm）
+- 过滤，保留微球和滤液
+<!--rehype:className=style-timeline-->
+
+### 浓度测试-显色反应
+
+- 去离子水洗，润洗后，移取1mL待测样品
+- 移取5mL 6M盐酸
+- 移液枪移取0.5mL SnCl2和0.5mL 20% NH4SCH
+- 静置20min
+- 移取5mL乙酸乙酯
+- 静置10min
+<!--rehype:className=style-timeline-->
+
+### 分光光度准备
+
+- 前往310，带乙酸乙酯，比色皿，样品，手纸，吸管
+- 电脑开机设备开机
+- 电脑启动UV Probe
+- 基线800-200，自动调零
+- 放入乙酸乙酯样品于前后端
+
+    <img
+    src="assets/26041901.png"
+    alt="alt text"
+    width="200"
+    />
+- 基线800-200，自动调零
+- Ctrl-M 附件 6连池
+- 进入【光度测量】
+- 进入【自动调零】
+<!--rehype:className=style-timeline-->
+
+### 分光光度测量
+
+- 打开`E:/lele/铼标准曲线`
+- 样品表写id写1，2，3...
+
+    <img
+    src="assets/26041902.jpg"
+    alt="alt text"
+    width="200"
+    />
+- 【读取Unk】
+<!--rehype:className=style-timeline-->
diff --git a/readme.md b/readme.md
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+++ b/readme.md
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+flt QRH
+===
+
+[实验](./docs/实验.md) <!--rehype:style=background:rgb(79 91 147);-->
+<!--rehype:class=home-card-->
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